Stress Corrosion Cracking Detection of Sensitized Stainless Steel 304 in Chloride Media by Using Electrochemical Impedance Spectroscopy (EIS)

نویسندگان

  • A. Sardashti Department of Chemistry, Islamic Azad University, North Tehran Branch
  • B. Adib Department of Chemistry, Islamic Azad University, North Tehran Branch
  • J. Neshati Corrosion Department, Research Institute of Petroleum Industry (RIPI)
چکیده مقاله:

Electrochemical impedance spectroscopy (EIS) was used to detect stress corrosion cracking (SCC) in stainless steel 304 alloy exposed to an aqueous environment at 120 °C. Stainless steel 304 alloy as u-bend was tested in the solution that contains 40 weight percent of magnesium chloride. U-bended samples were prepared according to ASTM G30. EIS measurements were always performed simultaneously on u-bend samples under stress and non-stress conditions. The results indicate that changes in phase shift versus time could be related to the stress corrosion cracking process. Stress corrosion cracking is detectable at a frequency of 23.95 Hz. EIS measurement can be used for SCC monitoring in u-bend samples. Finally, analysis of the fracture surface by using metallographic and SEM techniques confirmed the EIS results.

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عنوان ژورنال

دوره 2  شماره 1

صفحات  55- 60

تاریخ انتشار 2012-01-11

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